HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Succinamide → 1-(2-Bromoethyl)pyrrolidine-2,5-dione
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Succinamide | HCID 8036 | — |
| Edukt | 1,1-Dibromoethane | HCID 11201 | — |
| Edukt | Potassium Carbonate | HCID 11430 | — |
| Lösungsmittel | Methyl Ethyl Ketone | HCID 6569 | — |
| Produkt | 1-(2-Bromoethyl)pyrrolidine-2,5-dione | HCID 13561395 | — |
Reaktionsschritte
49.5 g of succinamide was dissolved in 750 ml of 2-butanone under heating. 187.9 g of dibromoethane and 138 g of anhydrous potassium carbonate were added to the solution and the mixture was heated under reflux for 9.5 h.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04801603 |
| Quelldatensatz | uspto-grants-1989_01 |
| ORD ID | ord-c828f9b75a7a408abe6987fc6ce65114 |
| Quellennotiz | uspto-grants-1989_01 |