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HRID2292130

反应详情

EQUATION

反应方程式

HRID 2292130 的结构方程式

REACTANTS

反应物

3
结构：NC(=O)CCC(N)=O
HCID8036

Butanediamide

C4H8N2O2

结构：CC(Br)Br
HCID11201

Ethylidene bromide

C2H4Br2

结构：O=C([O-])[O-].[K+].[K+]
HCID11430

Potassium Carbonate

CK2O3

PRODUCTS

生成物

1
结构：O=C1CCC(=O)N1CCBr
HCID13561395

1-(2-Bromoethyl)pyrrolidine-2,5-dione

C6H8BrNO2

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCC(C)=O
溶剂HCID6569

Methyl ethyl ketone

C4H8O

PROCEDURE

实验过程

49.5 g of succinamide was dissolved in 750 ml of 2-butanone under heating. 187.9 g of dibromoethane and 138 g of anhydrous potassium carbonate were added to the solution and the mixture was heated under reflux for 9.5 h.

WORKUP

后处理

  1. temperatureunder heating
  2. temperaturethe mixture was heated
  3. temperatureunder reflux for 9.5 h.