HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
tert-Butyl methacrylate → 3-[tris(trimethylsilyloxy)silyl]propyl methacrylate t-butyl methacrylate 5-oxo-4-oxatricyclo[4.2.1.03,7]nonan-2-yl Methacrylate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | tert-Butyl methacrylate | HCID 11448 | — |
| Edukt | 3-(Tris(trimethylsiloxy)silyl)propyl methacrylate | HCID 123371 | — |
| Edukt | 1,4,4-Trimethyl-4-silacyclohexyl methacrylate | HCID 18381205 | — |
| Produkt | 3-[tris(trimethylsilyloxy)silyl]propyl methacrylate t-butyl methacrylate 5-oxo-4-oxatricyclo[4.2.1.03,7]nonan-2-yl Methacrylate | HCID 70157708 | — |
Reaktionsschritte
A copolymer was synthesized as in Polymer Synthesis Example 1 except that 3-[tris(trimethylsilyloxy)silyl]propyl methacrylate and t-butyl methacrylate were used instead of 1,4,4-trimethyl-4-silacyclohexyl methacrylate. The polymer was confirmed by the light scattering method to have a weight average molecular weight of 13,000 g/mol and by the GPC elution curve to have a dispersity (Mw/Mn) of 1.78. By 1H-NMR analysis, the copolymer was found to contain the components in a ratio of approximately 2:5:3.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06492089B2 |
| Quelldatensatz | uspto-grants-2002_12 |
| ORD ID | ord-f11f81e9aa554f2595304d658ef37647 |
| Quellennotiz | uspto-grants-2002_12 |