Phenyl Isothiocyanate → 3-(2-furyl)-4-phenyl-5-{[4-(trifluoromethyl)benzyl]thio}-4H-1,2,4-triazole
Reaktionsgleichung
[O:1]1[CH:5]=[CH:4][CH:3]=[C:2]1[C:6]([NH:8][NH2:9])=O.[C:10]1([N:16]=[C:17]=[S:18])[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=1.[F:19][C:20]([F:30])([F:29])[C:21]1[CH:28]=[CH:27][C:24]([CH2:25]Br)=[CH:23][CH:22]=1>>[O:1]1[CH:5]=[CH:4][CH:3]=[C:2]1[C:6]1[N:16]([C:10]2[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=2)[C:17]([S:18][CH2:25][C:24]2[CH:23]=[CH:22][C:21]([C:20]([F:19])([F:29])[F:30])=[CH:28][CH:27]=2)=[N:9][N:8]=1Komponenten
4
Versuchsvorschrift
This compound was synthesized using the same methodology as described in Example 1 above, using 2-furancarboxylic acid hydrazide, phenyl isothiocyanate and 4-trifluoromethylbenzyl bromide as the starting materials. (M+H)+−402.