Acryloyl chloride → 3,5-Dihydroxy-1-adamantyl methacrylate

HRID 2305280

Reaktionsgleichung

[C:1]12([OH:13])[CH2:10][C:5]3([OH:11])[CH2:6][CH:7]([CH2:9][C:3]([OH:12])([CH2:4]3)[CH2:2]1)[CH2:8]2.[C:14](Cl)(=[O:18])[C:15]([CH3:17])=[CH2:16].C12(O)CC3CC(CC(O)(C3)C1)C2.C(Cl)(=O)C=C>>[OH:13][C:1]12[CH2:10][C:5]3([O:11][C:14](=[O:18])[C:15]([CH3:17])=[CH2:16])[CH2:6][CH:7]([CH2:9][C:3]([OH:12])([CH2:4]3)[CH2:2]1)[CH2:8]2

Komponenten

Edukt 4

HCID 13140Acryloyl chloride

HCID 13528Methacryloyl chloride

HCID 5738291,3-Adamantanediol

HCID 98990221,3,5-Adamantanetriol

Produkt 1

HCID 130073943,5-Dihydroxy-1-adamantyl methacrylate

Versuchsvorschrift

The title compound was prepared in the same manner as in Production Example 6, except that 1,3,5-adamantanetriol and methacrylic chloride were used instead of 1,3-adamantanediol and acrylic chloride, respectively.

Quellen und Nachweise

ORD-Eintrag: ord-3333ea1e07474971bc63cb7683b11d73
Quelldatensatz: uspto-grants-2002_08
DOI: 10.6084/m9.figshare.5104873.v1
Patentnummer: US06440636B1

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