Butyl iodide → HCID 17902130, Verbindung

Reaktionsgleichung

[N+:1]([C:4]1[CH:5]=[C:6]2[C:10](=[CH:11][CH:12]=1)[N:9]=[C:8]([CH3:13])[C:7]2([CH3:15])[CH3:14])([O-:3])=[O:2].[I:16][CH2:17][CH2:18][CH2:19][CH3:20]>>[I-:16].[CH2:17]([N+:9]1[C:10]2[C:6](=[CH:5][C:4]([N+:1]([O-:3])=[O:2])=[CH:12][CH:11]=2)[C:7]([CH3:15])([CH3:14])[C:8]=1[CH3:13])[CH2:18][CH2:19][CH3:20]

Komponenten

Edukt 2

HCID 10962Butyl iodide

HCID 975513H-Indole, 2,3,3-trimethyl-5-nitro-

Produkt 1

HCID 17902130HCID 17902130, Verbindung

Versuchsvorschrift

5-Nitro-2,3,3-trimethylindole (250 mg, 1.22 mmol) and iodobutane (10 ml, 16.17 g, 87.87 mmol) were mixed and heated to reflux for 16hrs. The solvent was removed and the impure material stored at−20° C. for use in later reactions.

Aufarbeitung

temperatureheated
temperatureto reflux for 16hrs
customThe solvent was removed
custom20° C.

Quellen und Nachweise

ORD-Eintrag: ord-0bfeec58765445f6a35d1b465bfbc39c
Quelldatensatz: uspto-grants-2004_12
DOI: 10.6084/m9.figshare.5104873.v1
Patentnummer: US06828116B1

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