Methyl iodide → 2-[(2-Methoxy-3-octadecyloxypropyl)sulfonyl]ethyltrimethylammonium iodide

HRID 231264Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 231264
[CH3:1][O:2][CH:3]([CH2:13][O:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH2:30][CH2:31][CH3:32])[CH2:4][S:5]([CH2:8][CH2:9][N:10]([CH3:12])[CH3:11])(=[O:7])=[O:6].[CH3:33][I:34]>CCOCC>[I-:34].[CH3:1][O:2][CH:3]([CH2:13][O:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH2:30][CH2:31][CH3:32])[CH2:4][S:5]([CH2:8][CH2:9][N+:10]([CH3:33])([CH3:12])[CH3:11])(=[O:6])=[O:7]

Komponenten

4

Edukt 2

HCID 6328Methyl iodideHCID 144982652-[(2-Methoxy-3-octadecyloxypropyl)sulfonyl]ethyldimethylamine

Produkt 1

HCID 144982482-[(2-Methoxy-3-octadecyloxypropyl)sulfonyl]ethyltrimethylammonium iodide

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 3283Diethyl EtherLösungsmittel

Versuchsvorschrift

In 5 ml of ether is dissolved 0.24 g of 2-[(2-methoxy-3-octadecyloxypropyl)sulfonyl]ethyldimethylamine to which is added 1 ml of methyl iodide. The solution is then stirred at room temperature for 2 days. The reaction liquid is concentrated under reduced pressure and the residue is treated with methanol to give 275 mg of the captioned compound as powder.

Aufarbeitung

  1. customThe reaction liquid
  2. concentrationis concentrated under reduced pressure
  3. additionthe residue is treated with methanol

Quellen und Nachweise

ORD-Eintrag
ord-c41443b41d0f4024954fde2ad444d8d1
Quelldatensatz
uspto-grants-1989_07
Patentnummer
US04845219

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