HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Nitric Acid → 4-Tert-butyl-1-methyl-2-nitrobenzene
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Nitric Acid | HCID 944 | — |
| Edukt | Sulfuric Acid | HCID 1118 | — |
| Edukt | 4-tert-Butyltoluene | HCID 7390 | — |
| Lösungsmittel | Water | HCID 962 | — |
| Produkt | 4-Tert-butyl-1-methyl-2-nitrobenzene | HCID 10954415 | — |
Reaktionsschritte
Nitration was performed as described in General Method 12 using tert-butyl-4-methylbenzene (25 g), concentrated H2SO4 (92 g), 70% HNO3 (82 g), and H2O (25 g). The crude product was purified via distillation under vacuum.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06852711B2 |
| Quelldatensatz | uspto-grants-2005_02 |
| ORD ID | ord-28047e1787ec4cb588412d11eb80d13c |
| Quellennotiz | uspto-grants-2005_02 |