Tetrahydrofuran → HCID 22033037, Verbindung

HRID 2353491Notizen

Reaktionsgleichung

[CH2:1]([O:8][CH:9](O)[CH2:10][CH2:11][CH3:12])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.C(N(CC)CC)C.[CH3:21][S:22](Cl)(=[O:24])=[O:23].C1C[O:29]CC1>>[CH3:21][S:22]([O:24][CH2:12][CH2:11][CH2:10][CH2:9][O:8][CH2:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1)(=[O:29])=[O:23]

Komponenten

Edukt 4

HCID 8028Tetrahydrofuran

HCID 8471Triethylamine

HCID 31297Methanesulfonyl chloride

HCID 198665521-Benzyloxy-1-butanol

Produkt 1

HCID 22033037HCID 22033037, Verbindung

Versuchsvorschrift

The 1-benzyloxy-1-butanol (Aldrich, 0.22 g, 1.2 mmol), triethylamine (0.56 mL, 4.1 mmol), and methanesulfonyl chloride (0.15 mL, 1.9 mmol) in 10 mL THF were processed as described in Example 1C to give the title compound that was used directly in the next reaction.

Quellen und Nachweise

ORD-Eintrag: ord-162a22e97d90400694bed12d79f77ce3
Quelldatensatz: uspto-grants-2010_07
DOI: 10.6084/m9.figshare.5104873.v1
Patentnummer: US07750039B2

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