Water → 1-Methyl 2,6-dichloro-1,4-benzenedicarboxylate
Reaktionsgleichung
[Cl:1][C:2]1[CH:10]=[C:9]([C:11]([O:13]C)=[O:12])[CH:8]=[C:7]([Cl:15])[C:3]=1[C:4]([OH:6])=[O:5].[OH-].[Na+].O.O1CCC[CH2:20]1>Cl.C(OCC)(=O)C>[CH3:20][O:6][C:4](=[O:5])[C:3]1[C:2]([Cl:1])=[CH:10][C:9]([C:11]([OH:13])=[O:12])=[CH:8][C:7]=1[Cl:15]Komponenten
7
Edukt 4
Produkt 1
Reagenzien, Katalysatoren, Lösungsmittel 2
Versuchsvorschrift
The mixture of 560 mg of 2,6-dichloro-4-methoxycarbonyl benzoic acid, 85 mg of sodium hydroxide, 5 ml of water and 5 ml of tetrahydrofuran was stirred for 1 hour. The mixture was diluted with 1N hydrochloric acid and treated by an ordinary method using ethyl acetate as an extractant to obtain the title compound.
Aufarbeitung
- additiontreated by an ordinary method
Quellen und Nachweise
- ORD-Eintrag
- ord-04fb529a1f6d4feda0e453ccaadbedfd
- Quelldatensatz
- uspto-grants-2010_07
- Patentnummer
- US07759388B2
Notizen zur Reaktion
Wird geladen…