Dichloromethane → Chloromethyl 2-cyanoethylether
Reaktionsgleichung
CS[CH2:3][CH:4]([C:14]#[N:15])[CH2:5][O:6][CH2:7][CH:8]([C:12]#[N:13])CSC.S(Cl)([Cl:19])(=O)=O.[CH2:21]([Cl:23])Cl>>[Cl:19][CH2:3][CH:4]([C:14]#[N:15])[CH2:5][O:6][CH2:7][CH:8]([C:12]#[N:13])[CH2:21][Cl:23]Komponenten
4
Versuchsvorschrift
Methylthiomethyl 2-cyanoethylether (3.3 g, 25 mmol) was dissolved in 70 mL of methylene chloride, and 2 mL of sulfuryl chloride (25 mmol) was added dropwise, and the reaction was further performed at room temperature for 1 hour.
Quellen und Nachweise
- ORD-Eintrag
- ord-9eef10283fa44218be2307d7308f4d43
- Quelldatensatz
- uspto-grants-2014_04
- Patentnummer
- US08691970B2
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