1,4-Butanediol → 1,4-Butanediol silicate

Reaktionsgleichung

[Si:1]([OH:5])([OH:4])([OH:3])[OH:2].[CH2:6]([OH:11])[CH2:7][CH2:8][CH2:9][OH:10].C(=O)([O-])[O-].[Na+].[Na+]>>[Si:1]([OH:5])([OH:4])([OH:3])[OH:2].[CH2:6]([OH:11])[CH2:7][CH2:8][CH2:9][OH:10]

Komponenten

Edukt 3

HCID 80641,4-Butanediol2×

HCID 10340Sodium Carbonate

HCID 14942Orthosilicic acid

Produkt 1

HCID 867357831,4-Butanediol silicate

Versuchsvorschrift

About 3 parts by weight of fine granular silicic acid gel, 3 parts by weight of 1,4-butanediol and 0.5 part by weight of sodium carbonate are mixed then heated to just below the boiling point of 1,4-butanediol for 20 to 60 minutes, thereby producing a light tan powder, 1,4-butanediol silicate.

Quellen und Nachweise

ORD-Eintrag: ord-67d512dba8be498ab8be5fd77f21a56f
Quelldatensatz: uspto-grants-1979_06
DOI: 10.6084/m9.figshare.5104873.v1
Patentnummer: US04159369

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