1-Phenylpiperazine → (4-Methanesulfonyl-biphenyl-2-yl)-(4-phenyl-piperazin-1-yl)-methanone

HRID 2374266

Reaktionsgleichung

Reaktionsgleichung von HRID 2374266
[C:1]1([N:7]2[CH2:12][CH2:11][NH:10][CH2:9][CH2:8]2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[CH3:13][S:14]([C:17]1[CH:18]=[C:19]([C:29](O)=[O:30])[C:20]([C:23]2[CH:28]=[CH:27][CH:26]=[CH:25][CH:24]=2)=[CH:21][CH:22]=1)(=[O:16])=[O:15]>>[CH3:13][S:14]([C:17]1[CH:22]=[CH:21][C:20]([C:23]2[CH:28]=[CH:27][CH:26]=[CH:25][CH:24]=2)=[C:19]([C:29]([N:10]2[CH2:11][CH2:12][N:7]([C:1]3[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=3)[CH2:8][CH2:9]2)=[O:30])[CH:18]=1)(=[O:15])=[O:16]

Komponenten

3

Edukt 2

HCID 70961-PhenylpiperazineHCID 574452544-(methylsulfonyl)-Biphenyl-2-carboxylic acid

Produkt 1

HCID 59853751(4-Methanesulfonyl-biphenyl-2-yl)-(4-phenyl-piperazin-1-yl)-methanone

Versuchsvorschrift

The title compound was prepared according to the procedure E described for Example 9 from phenyl piperazine [189457-54-3] and 4-Methanesulfonyl-biphenyl-2-carboxylic acid (Example V). MS (ISP): 421.3 MH+.

Quellen und Nachweise

ORD-Eintrag
ord-c8e1237ddabd4ecc84762ee539f1b69b
Quelldatensatz
uspto-grants-2008_12
Patentnummer
US07462617B2

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