Glycine → Magnesium Glycinate

HRID 2397423

Reaktionsgleichung

Reaktionsgleichung von HRID 2397423
C(=O)([O-])[O-].[Mg+2:5].[NH2:6][CH2:7][C:8]([OH:10])=[O:9].[N+]([O-])([O-])=O>O>[NH2:6][CH2:7][C:8]([O-:10])=[O:9].[Mg+2:5].[NH2:6][CH2:7][C:8]([O-:10])=[O:9]

Komponenten

5

Edukt 3

HCID 750GlycineHCID 943NitrateHCID 11029Magnesium Carbonate

Produkt 1

HCID 84645Magnesium Glycinate

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 962WaterLösungsmittel

Versuchsvorschrift

Magnesium glycinate was prepared by reacting 1.8 g. of basic magnesium carbonate (26.1% Mg) with 3 g. of glycine in 30 g. of water, while agitating at 75° C. for one half hour. To the cooled slurry was added 50 g. of zirconyl nitrate solution [ZrO(NO3)2 ; 4.27% Zr] with agitation. The resultant clear solution had a pH of 3.2. The product was oven-dried at 55° C. under a vacuum of 35 cm. of Hg and found to contain 22.8% Zr, 4.79% Mg and 30.6% glycine.

Aufarbeitung

  1. additionTo the cooled slurry was added 50 g
  2. customThe product was oven-dried at 55° C. under a vacuum of 35 cm. of Hg

Quellen und Nachweise

ORD-Eintrag
ord-2816f9889ed74060b14625313a9c79ff
Quelldatensatz
uspto-grants-1977_05
Patentnummer
US04021536

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