Glycine → Magnesium Glycinate

HRID 2397424

Reaktionsgleichung

Reaktionsgleichung von HRID 2397424
C(=O)([O-])[O-].[Mg+2:5].[NH2:6][CH2:7][C:8]([OH:10])=[O:9].OCl>O>[NH2:6][CH2:7][C:8]([O-:10])=[O:9].[Mg+2:5].[NH2:6][CH2:7][C:8]([O-:10])=[O:9]

Komponenten

5

Edukt 3

HCID 750GlycineHCID 11029Magnesium CarbonateHCID 24341Hypochlorous Acid

Produkt 1

HCID 84645Magnesium Glycinate

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 962WaterLösungsmittel

Versuchsvorschrift

Magnesium glycinate was prepared by reacting 3 g. of basic magnesium carbonate (26.1% Mg) with 5 g. of glycine in 40 g. of H2O, while agitating at 75° C. for one half hour. To the cooled slurry was added 100 g. of 33-1/3% zirconyl hydroxychloride solution (4.4% Zr) with agitation. After 15 minutes of stirring, the solution cleared and had a pH of 3.4. The product was oven-dried at 50° C. under a vacuum of 35 cm. of Hg, and found to contain 2.06% Mg, 36.9% Zr, and 13.1% glycine.

Aufarbeitung

  1. additionTo the cooled slurry was added 100 g
  2. customThe product was oven-dried at 50° C. under a vacuum of 35 cm. of Hg

Quellen und Nachweise

ORD-Eintrag
ord-47e92070f7184e29beaf50a9e45223c5
Quelldatensatz
uspto-grants-1977_05
Patentnummer
US04021536

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