2,2,2-Trifluoroethanol → 2,2,2-Trifluoroethyl sulfamate

HRID 2405773Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 2405773
C1([O:4][S:5](=[O:8])(=[O:7])[NH2:6])CC1.[F:9][C:10]([F:14])([F:13])[CH2:11][OH:12]>>[F:9][C:10]([F:14])([F:13])[CH2:11][NH:6][S:5](=[O:8])(=[O:7])[O-:4].[F:9][C:10]([F:14])([F:13])[CH2:11][O:12][S:5](=[O:7])(=[O:4])[NH2:6]

Komponenten

4

Edukt 2

HCID 64092,2,2-TrifluoroethanolHCID 57785190Cyclopropyl sulfamate

Produkt 2

HCID 133603552,2,2-Trifluoroethyl sulfamateHCID 18378142HCID 18378142, Verbindung

Versuchsvorschrift

2,2,2-Trifluoroethylsulfamate was synthesized according to the method presented in the synthesis of sulfamic acid cyclopropyl ester in Example 1 with the exception of utilizing 2,2,2-trifluoroethylalcohol to obtain sulfamic acid 2,2,2-trifluoro-ethyl ester.

Quellen und Nachweise

ORD-Eintrag
ord-37a98e57a5fc489ea84d6011c6b72303
Quelldatensatz
uspto-grants-2014_08
Patentnummer
US08809267B2

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