HCID 68613896, Verbindung → 2-Methoxy-7-quinolinamine
Reaktionsgleichung
[CH3:1][O:2][C:3]1[CH:12]=[CH:11][C:10]2[C:5](=[CH:6][C:7]([N+:13]([O-])=O)=[CH:8][CH:9]=2)[N:4]=1>[Pd].CO>[CH3:1][O:2][C:3]1[CH:12]=[CH:11][C:10]2[C:5](=[CH:6][C:7]([NH2:13])=[CH:8][CH:9]=2)[N:4]=1Komponenten
4
Edukt 1
Produkt 1
Reagenzien, Katalysatoren, Lösungsmittel 2
Versuchsvorschrift
A methanol (10 ml) solution containing 2-methoxy-7-nitroquinoline (33 mg) obtained in the 1st step was prepared and subjected to a hydrogenation reaction (60° C.; 50 bar; flow rate: 1 ml/min; 10% Pd/C) using H-cube™. Then, the solvent was distilled away under reduced pressure, and a purple solid of 2-methoxyquinolin-7-amine (28 mg) was thus obtained.
Aufarbeitung
- customobtained in the 1st step
- customwas prepared
- distillationThen, the solvent was distilled away under reduced pressure
Quellen und Nachweise
- ORD-Eintrag
- ord-300ad33cc96842d7b1b05e7c8c479cb5
- Quelldatensatz
- uspto-grants-2014_08
- Patentnummer
- US08809371B2
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