Calcium Chloride → HCID 88641856, Verbindung

HRID 2413831Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 2413831
[CH3:1][C:2]1[CH:18]=[C:17]([CH3:19])[CH:16]=[C:15]([CH3:20])[C:3]=1[C:4]([P:6]([C:9]1[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=1)(=[O:8])[O-:7])=[O:5].[Na+].[Cl-].[Ca+2:23].[Cl-]>O>[CH3:1][C:2]1[CH:18]=[C:17]([CH3:19])[CH:16]=[C:15]([CH3:20])[C:3]=1[C:4]([P:6]([C:9]1[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=1)(=[O:7])[O-:8])=[O:5].[CH3:1][C:2]1[CH:18]=[C:17]([CH3:19])[CH:16]=[C:15]([CH3:20])[C:3]=1[C:4]([P:6]([C:9]1[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=1)(=[O:7])[O-:8])=[O:5].[Ca+2:23]

Komponenten

4

Edukt 2

HCID 5284359Calcium ChlorideHCID 23690966Phosphinic acid, P-phenyl-P-(2,4,6-trimethylbenzoyl)-, sodium salt (1:1)

Produkt 1

HCID 88641856HCID 88641856, Verbindung

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 962WaterLösungsmittel

Versuchsvorschrift

15 parts by weight of the sodium salt of Example 1 were dissolved in 75 parts by weight of water, and 125 parts by volume of a 10% strength aqueous calcium chloride solution were added a little at a time to this solution. The resulting precipitate was filtered off under suction, washed with water and dried in a drying oven under reduced pressure at 50° C., and 14.7 parts by weight of product were obtained.

Aufarbeitung

  1. additionwere added a little at a time to this solution
  2. filtrationThe resulting precipitate was filtered off under suction
  3. washwashed with water
  4. customdried in a drying oven under reduced pressure at 50° C.
  5. custom14.7 parts by weight of product were obtained

Quellen und Nachweise

ORD-Eintrag
ord-bf4042638b344e4c9bd77cf614fc03a9
Quelldatensatz
uspto-grants-1988_01
Patentnummer
US04719297

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