1,3-Dibromopropane → Ethyl 1-pyridin-3-ylcyclobutane-1-carboxylate

HRID 2424928

Reaktionsgleichung

Reaktionsgleichung von HRID 2424928
[N:1]1[CH:6]=[CH:5][CH:4]=[C:3]([CH2:7][C:8]([O:10][CH2:11][CH3:12])=[O:9])[CH:2]=1.Br[CH2:14][CH2:15][CH2:16]Br>>[N:1]1[CH:6]=[CH:5][CH:4]=[C:3]([C:7]2([C:8]([O:10][CH2:11][CH3:12])=[O:9])[CH2:16][CH2:15][CH2:14]2)[CH:2]=1

Komponenten

3

Edukt 2

HCID 80011,3-DibromopropaneHCID 96490Ethyl 3-pyridylacetate

Produkt 1

HCID 67246748Ethyl 1-pyridin-3-ylcyclobutane-1-carboxylate

Versuchsvorschrift

Prepared in a similar manner to that described above by reacting ethyl 2-pyridin-3-ylacetate with 1,3-dibromopropane to give ethyl 1-pyridin-3-ylcyclobutane-1-carboxylate which was then hydrogenated to give the desired compound as a brown oil (quantitative reaction).

Aufarbeitung

  1. customPrepared in a similar manner to that

Quellen und Nachweise

ORD-Eintrag
ord-f374677e9bf0408cab463ad44f34a638
Quelldatensatz
uspto-grants-2011_06
Patentnummer
US07964618B2

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