4-Nitrobenzoic Acid → N-[3-(methylsulfanyl)phenyl]-4-nitrobenzamide
Reaktionsgleichung
[CH3:1][S:2][C:3]1[CH:4]=[C:5]([CH:7]=[CH:8][CH:9]=1)[NH2:6].[N+:10]([C:13]1[CH:21]=[CH:20][C:16]([C:17](O)=[O:18])=[CH:15][CH:14]=1)([O-:12])=[O:11]>>[N+:10]([C:13]1[CH:14]=[CH:15][C:16]([C:17]([NH:6][C:5]2[CH:7]=[CH:8][CH:9]=[C:3]([S:2][CH3:1])[CH:4]=2)=[O:18])=[CH:20][CH:21]=1)([O-:12])=[O:11]Komponenten
3
Versuchsvorschrift
Using 3-methylthioaniline (1.40 ml, 11.0 mmol) and 4-nitrobenzoic acid (1.67 g, 10.0 mmol), the procedure of Reference Example 16 was repeated to obtain 2.46 g (85.2%) of the title compound in the form of yellow powder.
Quellen und Nachweise
- ORD-Eintrag
- ord-bac4f35022814f6eaa0f9cad74b4ef8c
- Quelldatensatz
- uspto-grants-1998_03
- Patentnummer
- US05728835
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