4-Nitrobenzoic Acid → N-(4-Methylphenyl)-4-nitrobenzamide
Reaktionsgleichung
[NH2:1][C:2]1[CH:7]=[CH:6][C:5]([CH3:8])=[CH:4][CH:3]=1.[N+:9]([C:12]1[CH:20]=[CH:19][C:15]([C:16]([OH:18])=O)=[CH:14][CH:13]=1)([O-:11])=[O:10]>>[N+:9]([C:12]1[CH:13]=[CH:14][C:15]([C:16]([NH:1][C:2]2[CH:7]=[CH:6][C:5]([CH3:8])=[CH:4][CH:3]=2)=[O:18])=[CH:19][CH:20]=1)([O-:11])=[O:10]Komponenten
3
Versuchsvorschrift
Using p-toluidine (1.19 g, 11.0 mmol) and 4-nitrobenzoic acid (1.77 g, 10.5 mmol), the procedure of Reference Example 16 was repeated to obtain 2.68 g (99.6%) of the title compound in the form of light yellow needle crystals.
Quellen und Nachweise
- ORD-Eintrag
- ord-225d5fd599ed478295e732ac8190f2ec
- Quelldatensatz
- uspto-grants-1998_03
- Patentnummer
- US05728835
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