(Phenylthio)acetic acid → (Phenylthio)acetyl chloride

HRID 246816

Reaktionsgleichung

Reaktionsgleichung von HRID 246816
[C:1]1([S:7][CH2:8][C:9]([OH:11])=O)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.C(Cl)(=O)C([Cl:15])=O>C1(C)C=CC=CC=1>[C:1]1([S:7][CH2:8][C:9]([Cl:15])=[O:11])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1

Komponenten

4

Edukt 2

HCID 59541(Phenylthio)acetic acidHCID 65578Oxalyl chloride

Produkt 1

HCID 4063350(Phenylthio)acetyl chloride

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 1140TolueneLösungsmittel

Versuchsvorschrift

To a solution of 5.0 g of (phenylthio)acetic acid in 20 ml of toluene under nitrogen was added 5.2 ml of oxalyl chloride in four portions. The solution was stirred at room temperature for about twenty hours and then concentrated in vacuo to the oily title compound, which was used in subsequent reactions without further purificaton or characterization.

Aufarbeitung

  1. concentrationconcentrated in vacuo to the oily title compound, which

Quellen und Nachweise

ORD-Eintrag
ord-9ef97c2bf9824e38b8c136f32ff6aa57
Quelldatensatz
uspto-grants-1987_11
Patentnummer
US04704386

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