HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Ethanol → 3-(1-Ethoxy-1-phenyl-methylidene)-2-indolinone
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Ethanol | HCID 702 | — |
| Edukt | Sodium Hydroxide | HCID 14798 | — |
| Edukt | 1-Acetyl-3-(1-ethoxy-1-phenylmethylidene}-2-indolinone | HCID 54237888 | — |
| Lösungsmittel | Water | HCID 962 | — |
| Produkt | 3-(1-Ethoxy-1-phenyl-methylidene)-2-indolinone | HCID 54037623 | — |
Reaktionsschritte
6.15 g (20 mmol) of 1-acetyl-3-(1-ethoxy-1-phenyl-methylidene)-2-indolinone are suspended in a little ethanol. 10 ml of 4N sodium hydroxide solution are added and the mixture is stirred for 1.5 hours at ambient temperature. After the addition of 100 ml of water the precipitate is suction filtered, washed with water and a little ether and dried at 80° C.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06855710B2 |
| Quelldatensatz | uspto-grants-2005_02 |
| ORD ID | ord-2873a7ec518c40c286dc86ec59daace2 |
| Quellennotiz | uspto-grants-2005_02 |