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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 24740Erstellt: 25. Oktober 2026

Ethanol → 3-(1-Ethoxy-1-phenyl-methylidene)-2-indolinone

https://huagongshe.com/reaction/24740

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktEthanolHCID 702—
EduktSodium HydroxideHCID 14798—
Edukt1-Acetyl-3-(1-ethoxy-1-phenylmethylidene}-2-indolinoneHCID 54237888—
LösungsmittelWaterHCID 962—
Produkt3-(1-Ethoxy-1-phenyl-methylidene)-2-indolinoneHCID 54037623—

Reaktionsschritte

6.15 g (20 mmol) of 1-acetyl-3-(1-ethoxy-1-phenyl-methylidene)-2-indolinone are suspended in a little ethanol. 10 ml of 4N sodium hydroxide solution are added and the mixture is stirred for 1.5 hours at ambient temperature. After the addition of 100 ml of water the precipitate is suction filtered, washed with water and a little ether and dried at 80° C.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS06855710B2
Quelldatensatzuspto-grants-2005_02
ORD IDord-2873a7ec518c40c286dc86ec59daace2
Quellennotizuspto-grants-2005_02