HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 249139Erstellt: 27. Oktober 2026
3-(2-Methylpropenyl)benzonitrile → 3-Isobutylbenzonitrile
https://huagongshe.com/reaction/249139
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | 3-(2-Methylpropenyl)benzonitrile | HCID 19024792 | — |
| Katalysator | Palladium | HCID 23938 | — |
| Lösungsmittel | Methanol | HCID 887 | — |
| Produkt | 3-Isobutylbenzonitrile | HCID 19024755 | 94% |
Reaktionsschritte
To a solution of 3-(2-methyl-1-propenyl)benzonitrile (5.80 g) in methanol (50 ml) was added 10% palladium on activated carbon (1 g), and the mixture was stirred under hydrogen atmosphere (3 atm) at 25° C. for 1 hour. The catalyst was filtered off and the filtrate was evaporated to give 3-isobutylbenzonitrile (5.52 g) as a pale yellow oil.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patentnummer | US05212320 |
|---|
| Quelldatensatz | uspto-grants-1993_05 |
|---|
| ORD ID | ord-d6481656cfa043db90ae1011ec48aef2 |
|---|
| Quellennotiz | uspto-grants-1993_05 |
|---|