Methyl Acrylate → Methyl 3-(3,5-dicyclohexyl-4-hydroxyphenyl)propionate

HRID 256101

Reaktionsgleichung

[CH:1]1([C:7]2[CH:12]=[CH:11][CH:10]=[C:9]([CH:13]3[CH2:18][CH2:17][CH2:16][CH2:15][CH2:14]3)[C:8]=2[OH:19])[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1.C([O-])(=O)C.[K+].[C:25]([O:29][CH3:30])(=[O:28])[CH:26]=[CH2:27]>>[CH:1]1([C:7]2[CH:12]=[C:11]([CH2:27][CH2:26][C:25]([O:29][CH3:30])=[O:28])[CH:10]=[C:9]([CH:13]3[CH2:14][CH2:15][CH2:16][CH2:17][CH2:18]3)[C:8]=2[OH:19])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6]1

Komponenten

Edukt 3

HCID 7294Methyl Acrylate

HCID 785402,6-Dicyclohexylphenol

HCID 517044Potassium Acetate

Produkt 1

HCID 20165247Methyl 3-(3,5-dicyclohexyl-4-hydroxyphenyl)propionate

Versuchsvorschrift

The yield of crude product is 1217 g. The crude product contains 800 g of product, 120 g of 2,6-dicyclohexylphenol, 27 g of potassium acetate and also oligomerised methyl acrylate.

Quellen und Nachweise

ORD-Eintrag: ord-f7c3b7b0cb204e44aba2036b882c5b01
Quelldatensatz: uspto-grants-1987_10
DOI: 10.6084/m9.figshare.5104873.v1
Patentnummer: US04699939

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