Diethyl Ether → 5-Norbornene-2-carboxylic acid

HRID 256805

Reaktionsgleichung

Reaktionsgleichung von HRID 256805
[C:1]([OH:5])(=[O:4])[CH:2]=[CH2:3].[CH:6]1[CH2:10][CH:9]=[CH:8]C=1.[CH2:11](OCC)C>>[CH:3]12[CH2:11][CH:10]([CH:9]=[CH:8]1)[CH2:6][CH:2]2[C:1]([OH:5])=[O:4]

Komponenten

4

Edukt 3

HCID 3283Diethyl EtherHCID 6581Acrylic AcidHCID 7612Cyclopentadiene

Produkt 1

HCID 789495-Norbornene-2-carboxylic acidAusbeute 82 %

Versuchsvorschrift

49.5 g of acrylic acid was added to 49.9 g of cyclopentadiene and 40 ml of diethyl ether, and a reaction was allowed to react at room temperature for 2 hr with stirring. After the completion of the reaction, the reaction mixture was concentrated and purified by distillation to give 78.0 g (yield: 82%) of an intended product.

Aufarbeitung

  1. customto react at room temperature for 2 hr
  2. customAfter the completion of the reaction
  3. concentrationthe reaction mixture was concentrated
  4. distillationpurified by distillation

Quellen und Nachweise

ORD-Eintrag
ord-27035d7ebe8f4b13943e774c599ac188
Quelldatensatz
uspto-grants-1993_11
Patentnummer
US05260257

Verknüpfte Notizen

Wird geladen…