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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 257376Erstellt: 25. Oktober 2026

Isopropyl iodide → 2-Fluoro-4-isopropoxy-1-nitrobenzene

https://huagongshe.com/reaction/257376

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktIsopropyl iodideHCID 6362—
EduktPotassium CarbonateHCID 11430—
Edukt3-Fluoro-4-nitrophenolHCID 520948—
LösungsmittelAcetoneHCID 180—
Produkt2-Fluoro-4-isopropoxy-1-nitrobenzeneHCID 1353865295,6%

Reaktionsschritte

By the method of Example 3, Step A, 23.15 g (0.147 mole) of 3-fluoro-4-nitrophenol and 29.92 g (0.175 mole) of 2-iodopropane were reacted in the presence of 20.73 g (0.150 mole) of anhydrous potassium carbonate in 450 mL of acetone, yielding 28.0 g of 4-isopropoxy-2-fluoronitrobenzene as an oil. The NMR was consistent with the proposed structure.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS05262390
Quelldatensatzuspto-grants-1993_11
ORD IDord-dd66cd547acf42eab2d7601f2c383cc7
Quellennotizuspto-grants-1993_11