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HRID257376

反应详情

EQUATION

反应方程式

HRID 257376 的结构方程式

REACTANTS

反应物

3
结构：CC(C)I
HCID6362

2-Iodopropane

C3H7I

结构：O=C([O-])[O-].[K+].[K+]
HCID11430

Potassium Carbonate

CK2O3

结构：O=[N+]([O-])c1ccc(O)cc1F
HCID520948

3-Fluoro-4-nitrophenol

C6H4FNO3

PRODUCTS

生成物

1
结构：CC(C)Oc1ccc([N+](=O)[O-])c(F)c1
HCID13538652

2-Fluoro-1-nitro-4-[(propan-2-yl)oxy]benzene

C9H10FNO3

收率 95.6%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CC(C)=O
溶剂HCID180

Acetone

C3H6O

PROCEDURE

实验过程

By the method of Example 3, Step A, 23.15 g (0.147 mole) of 3-fluoro-4-nitrophenol and 29.92 g (0.175 mole) of 2-iodopropane were reacted in the presence of 20.73 g (0.150 mole) of anhydrous potassium carbonate in 450 mL of acetone, yielding 28.0 g of 4-isopropoxy-2-fluoronitrobenzene as an oil. The NMR was consistent with the proposed structure.