Phenethyl bromide → 1-Phenyl-3-(3-ethyl-4-pyridyl)-propane

HRID 257468

Reaktionsgleichung

Reaktionsgleichung von HRID 257468
[CH2:1]([C:3]1[CH:4]=[N:5][CH:6]=[CH:7][C:8]=1[CH3:9])[CH3:2].[CH2:10](Br)[CH2:11][C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1>>[C:12]1([CH2:11][CH2:10][CH2:9][C:8]2[CH:7]=[CH:6][N:5]=[CH:4][C:3]=2[CH2:1][CH3:2])[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1

Komponenten

3

Edukt 2

HCID 7666Phenethyl bromideHCID 682543-Ethyl-4-methylpyridine

Produkt 1

HCID 197833001-Phenyl-3-(3-ethyl-4-pyridyl)-propaneAusbeute 92,8 %

Versuchsvorschrift

1.13 g (9.35 mmol) of 3-ethyl-4-methylpyridine and 1.73 g (9.35 mmol) of phenethyl bromide were reacted in the same manner as in Example 1. The reaction product was purified to obtain 1.95 g of the desired compound (yield: 92.8%). The resulting compound was identified as 1-phenyl-3-(3-ethyl-4-pyridyl)-propane (hereinafter referred to as compound by the following analytical results.

Aufarbeitung

  1. customThe reaction product was purified

Quellen und Nachweise

ORD-Eintrag
ord-576d78986f6c4ca5b5901520247931b6
Quelldatensatz
uspto-grants-1993_11
Patentnummer
US05262420

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