HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Glycerol → 1160173-26-1
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Glycerol | HCID 753 | — |
| Edukt | Water | HCID 962 | — |
| Edukt | Menthone | HCID 26447 | — |
| Edukt | Potassium bisulfate | HCID 516920 | — |
| Lösungsmittel | Toluene | HCID 1140 | — |
| Produkt | 1160173-26-1 | HCID 9964606 | — |
Reaktionsschritte
In a 2 l three-necked flask there are introduced 308 g of 1-menthone (2 mol), 276 g of glycerol (3 mol) and 5 g of potassium hydrogen sulphate in toluene. This mixture is refluxed in a water separator. After 7 hours, 42 g of water have separated. The mixture is neutralised and distilled.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05266592 |
| Quelldatensatz | uspto-grants-1993_11 |
| ORD ID | ord-5839718a228d4b68a1e5eee670bc279b |
| Quellennotiz | uspto-grants-1993_11 |