Butyric Acid → Heptafluorobutyric acid

HRID 259473

Reaktionsgleichung

Reaktionsgleichung von HRID 259473
[F:1][C:2]([F:13])([C:9]([F:12])([F:11])[F:10])[C:3]([F:8])([F:7])[C:4]([F:6])=[O:5].C(O)(=[O:18])CCC.C(OC(=O)CCC)(=O)CCC>>[F:10][C:9]([F:12])([F:11])[C:2]([F:13])([F:1])[C:3]([F:8])([F:7])[C:4]([OH:18])=[O:5].[C:4]([F:6])(=[O:5])[CH2:3][CH2:2][CH3:9]

Komponenten

5

Edukt 3

HCID 264Butyric AcidHCID 7798Butyric anhydrideHCID 67632Heptafluorobutyroyl fluoride

Produkt 2

HCID 9777Heptafluorobutyric acidHCID 68035Butanoyl fluoride

Versuchsvorschrift

The following run illustrates the metathetical reaction of impure heptafluorobutyryl fluoride with butyric acid in the presence of butyric anhydride to give heptafluorobutyric acid and butyryl fluoride and the recovery of products from the reaction mixture by fractional distillation.

Quellen und Nachweise

ORD-Eintrag
ord-f0fd27ea775447efb4ba9fb622217ab9
Quelldatensatz
uspto-grants-1977_07
Patentnummer
US04038310

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