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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 259545Erstellt: 25. Oktober 2026

Pyridine → N-(3-(Oxazolo[4,5-b]pyridin-2-yl)phenyl)acetamide

https://huagongshe.com/reaction/259545

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktPyridineHCID 1049—
EduktAcetic AnhydrideHCID 7918—
Edukt3-(Oxazolo[4,5-b]pyridin-2-yl)anilineHCID 611086—
LösungsmittelWaterHCID 962—
ProduktN-(3-(Oxazolo[4,5-b]pyridin-2-yl)phenyl)acetamideHCID 2995970—

Reaktionsschritte

A solution of 0.63 g. of 2-(3-aminophenyl)oxazolo[4,5-b]pyridine in 10 ml. of pyridine was treated with 0.35 ml. of acetic anhydride with stirring. After stirring over the weekend the mixture was diluted to 50 ml. with water. After stirring a short time and cooling, the precipitate was collected, washed with water and dried. Recrystallization from ethyl acetate gave 2-(3-acetamidophenyl)oxazolo[4,5-b]pyridine, m.p. 201.5°-202.5°.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS04038396
Quelldatensatzuspto-grants-1977_07
ORD IDord-9562b43195984e0c811e2b8a33049552
Quellennotizuspto-grants-1977_07