Benzene → Isobutylidenebenzhydrylamine

HRID 25972

Reaktionsgleichung

Reaktionsgleichung von HRID 25972
[CH:1](=O)[CH:2]([CH3:4])[CH3:3].[CH:6]([NH2:19])([C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1)[C:7]1[CH:12]=[CH:11][CH:10]=[CH:9][CH:8]=1.C1C=CC=CC=1>O>[CH:1](=[N:19][CH:6]([C:7]1[CH:12]=[CH:11][CH:10]=[CH:9][CH:8]=1)[C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1)[CH:2]([CH3:4])[CH3:3]

Komponenten

5

Edukt 3

HCID 241BenzeneHCID 6561IsobutyraldehydeHCID 7036Benzhydrylamine

Produkt 1

HCID 10657527Isobutylidenebenzhydrylamine

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 962WaterLösungsmittel

Versuchsvorschrift

14.4 parts of isobutyraldehyde was added to 36.6 parts of benzhydrylamine in 100 parts of dry benzene at room temperature with stirring. The cloudy mixture was heated to reflux with water-separation for 4 hours. On cooling the solution was filtered to remove a small amount of solid and evaporated to give isobutylidenebenzhydrylamine.

Aufarbeitung

  1. temperatureThe cloudy mixture was heated
  2. temperatureOn cooling the solution
  3. filtrationwas filtered
  4. customto remove a small amount of solid
  5. customevaporated

Quellen und Nachweise

ORD-Eintrag
ord-c6b653a08d6e4a9db8afca08018af3b1
Quelldatensatz
uspto-grants-1979_04
Patentnummer
US04147780

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