HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2-Methoxyisonicotinonitrile → (2-Methoxypyridin-4-yl)methanamine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2-Methoxyisonicotinonitrile | HCID 7204887 | — |
| Katalysator | Palladium | HCID 23938 | — |
| Lösungsmittel | Ethanol | HCID 702 | — |
| Produkt | (2-Methoxypyridin-4-yl)methanamine | HCID 16227983 | — |
Reaktionsschritte
A solution of 4-cyano-2-methoxypyridine (0.55 g, 4.1 mmol) in ethanol was hydrogenated at 60 psi H2 in the presence of 10% Pd/C (100 mg). After 3.5 h the catalyst was removed by filtration through Super-Gel and the liltrate evaporated to give the title compound as a foam.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05527819 |
| Quelldatensatz | uspto-grants-1996_06 |
| ORD ID | ord-3fa0020c6e9c4e56a9b2fcba963c000d |
| Quellennotiz | uspto-grants-1996_06 |