HRID260472

反应详情

EQUATION

反应方程式

HRID 260472 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

A solution of 4-cyano-2-methoxypyridine (0.55 g, 4.1 mmol) in ethanol was hydrogenated at 60 psi H2 in the presence of 10% Pd/C (100 mg). After 3.5 h the catalyst was removed by filtration through Super-Gel and the liltrate evaporated to give the title compound as a foam.

WORKUP

后处理

  1. customAfter 3.5 h the catalyst was removed by filtration through Super-Gel
  2. customthe liltrate evaporated