Bromine → 2-Bromo-5-hydroxyindan-1,3-dione
Reaktionsgleichung
[Br:1]Br.[OH:3][C:4]1[CH:5]=[C:6]2[C:10](=[CH:11][CH:12]=1)[C:9](=[O:13])[CH2:8][C:7]2=[O:14]>C(Cl)(Cl)Cl>[Br:1][CH:8]1[C:7](=[O:14])[C:6]2[C:10](=[CH:11][CH:12]=[C:4]([OH:3])[CH:5]=2)[C:9]1=[O:13]Komponenten
4
Edukt 2
Produkt 1
Reagenzien, Katalysatoren, Lösungsmittel 1
Reaktionsbedingungen
- Temperatur
- 50 °C
Versuchsvorschrift
0.02 mol bromine was added dropwise to a solution of 0.02 mol of 5-hydroxyindan-1,3-dione in 60 ml chloroform. The reaction mixture was agitated at 50° C. for 30 minutes and the precipitate obtained after evaporation of the solvent was recrystallised.
Aufarbeitung
- customthe precipitate obtained
- customafter evaporation of the solvent
- customwas recrystallised
Quellen und Nachweise
- ORD-Eintrag
- ord-ec428e74b4b74bc394aeb405307d4ac3
- Quelldatensatz
- uspto-grants-1997_07
- Patentnummer
- US05648381
Notizen zur Reaktion
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