Chlorotriethylsilane → 3-Triethylsilyl-2-oxazolidinone

HRID 268304

Reaktionsgleichung

Reaktionsgleichung von HRID 268304
[CH2:1]([Si:3]([CH2:7][CH3:8])([CH2:5][CH3:6])Cl)[CH3:2].[O:9]1[CH2:13][CH2:12][NH:11][C:10]1=[O:14]>>[CH2:1]([Si:3]([CH2:7][CH3:8])([CH2:5][CH3:6])[N:11]1[CH2:12][CH2:13][O:9][C:10]1=[O:14])[CH3:2]

Komponenten

3

Edukt 2

HCID 13819ChlorotriethylsilaneHCID 739492-Oxazolidinone

Produkt 1

HCID 214547763-Triethylsilyl-2-oxazolidinone

Versuchsvorschrift

Following the previous example, but replacing the trimethylchlorosilane with triethylchlorosilane (63.3 g; 0.42 mol) and operating under similar conditions, the result is the compound of the above heading; a colorless fluid liquid, obtained with a similar yield. 2-oxazolidinone, calculated: 42.82%; found; 42.70%. Distills at 100°C between 2 and 4 mm.

Aufarbeitung

  1. customa colorless fluid liquid, obtained with a similar yield
  2. distillationDistills at 100°C between 2 and 4 mm

Quellen und Nachweise

ORD-Eintrag
ord-158e83453e7449beb90a25edd87432d5
Quelldatensatz
uspto-grants-1976_03
Patentnummer
US03947465

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