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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 270065Erstellt: 25. Oktober 2026

Cyclopropylamine → HCID 28390698, Verbindung

https://huagongshe.com/reaction/270065

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktCyclopropylamineHCID 69828—
EduktMethyl 4-methoxysalicylateHCID 79523—
ProduktHCID 28390698HCID 28390698—

Reaktionsschritte

A suspension of methyl 2-hydroxy-4-methoxybenzoate (5.1 g, 28.0 mmol) in cyclopropyl amine 24 mL) was stirred at room temperature for 5 days. The volatiles were removed in vacuo and the residue was purified by silica gel flash chromatography (0-60% ethyl acetate in petroleum ether) to give the subtitled compound (1.8 g).

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS07449475B2
Quelldatensatzuspto-grants-2008_11
ORD IDord-28b3b4d48a0f4850b7c740c5ce9c9a29
Quellennotizuspto-grants-2008_11