HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Cyclopropylamine → HCID 28390698, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Cyclopropylamine | HCID 69828 | — |
| Edukt | Methyl 4-methoxysalicylate | HCID 79523 | — |
| Produkt | HCID 28390698 | HCID 28390698 | — |
Reaktionsschritte
A suspension of methyl 2-hydroxy-4-methoxybenzoate (5.1 g, 28.0 mmol) in cyclopropyl amine 24 mL) was stirred at room temperature for 5 days. The volatiles were removed in vacuo and the residue was purified by silica gel flash chromatography (0-60% ethyl acetate in petroleum ether) to give the subtitled compound (1.8 g).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07449475B2 |
| Quelldatensatz | uspto-grants-2008_11 |
| ORD ID | ord-28b3b4d48a0f4850b7c740c5ce9c9a29 |
| Quellennotiz | uspto-grants-2008_11 |