1-Cyano-2-ethoxy-2-methylaminoethylene → HCID 178483853, Verbindung

HRID 27091

Reaktionsgleichung

Reaktionsgleichung von HRID 27091
[CH3:1][C:2]1[N:3]=[CH:4][NH:5][C:6]=1[CH2:7][S:8][CH2:9][CH2:10][NH2:11].[C:12]([CH:14]=[C:15](OCC)[NH:16][CH3:17])#[N:13]>N1C=CC=CC=1>[C:12]([CH:14]=[C:15]([NH:16][CH3:17])[NH:11][CH2:10][CH2:9][S:8][CH2:7][C:6]1[NH:5][CH:4]=[N:3][C:2]=1[CH3:1])#[N:13]

Komponenten

4

Edukt 2

HCID 736832021-Cyano-2-ethoxy-2-methylaminoethyleneHCID 178433288HCID 178433288, Verbindung

Produkt 1

HCID 178483853HCID 178483853, Verbindung

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 1049PyridineLösungsmittel

Versuchsvorschrift

4-Methyl-5-[(2-aminoethyl)thiomethyl]imidazole (3.5 g) was added to a solution of 1-cyano-2-ethoxy-2-methylaminoethylene in pyridine (3.1 g) and the solution was stirred for 5 hours at 100°. The product was chromatographed on a column of neutral alumina with elution by chloroform/ethyl acetate (1:1) to give the title compound as a glass.

Aufarbeitung

  1. customThe product was chromatographed on a column of neutral alumina with elution by chloroform/ethyl acetate (1:1)

Quellen und Nachweise

ORD-Eintrag
ord-10944535e2734a209418e4008f02eba6
Quelldatensatz
uspto-grants-1980_09
Patentnummer
US04220652

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