4-Aminophenethyl alcohol → HCID 66732874, Verbindung

HRID 273424

Reaktionsgleichung

Reaktionsgleichung von HRID 273424
[NH2:1][C:2]1[CH:7]=[CH:6][C:5]([CH2:8][CH2:9][OH:10])=[CH:4][CH:3]=1.[C:11]([O-:14])(=O)[CH3:12].[Na+].Cl[C:17]1[C:30]2[C:29](=[O:31])[C:28]3[C:23](=[C:24]([OH:33])[CH:25]=[CH:26][C:27]=3[OH:32])[C:22](=[O:34])[C:21]=2[C:20](Cl)=[CH:19][CH:18]=1>Cl>[OH:10][CH2:9][CH2:8][C:5]1[CH:6]=[CH:7][C:2]([NH:1][C:17]2[C:30]3[C:29](=[O:31])[C:28]4[C:23](=[C:24]([OH:33])[CH:25]=[CH:26][C:27]=4[OH:32])[C:22](=[O:34])[C:21]=3[C:20]([NH:1][C:2]3[CH:7]=[CH:6][C:5]([CH2:12][CH2:11][OH:14])=[CH:4][CH:3]=3)=[CH:19][CH:18]=2)=[CH:3][CH:4]=1

Komponenten

5

Edukt 3

HCID 669044-Aminophenethyl alcoholHCID 760711,4-Dichloro-5,8-dihydroxyanthraquinoneHCID 517045Sodium Acetate

Produkt 1

HCID 66732874HCID 66732874, Verbindung

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 313Hydrochloric AcidLösungsmittel

Reaktionsbedingungen

Temperatur
120 °C

Versuchsvorschrift

100 g of 2-(4-aminopheny)-ethanol and 20 g of sodium acetate are introduced into a laboratory reaction apparatus and, at 120° C., 20 g of 1,4-dichloro-5,8-dihydroxyanthraquinone are added thereto. The reaction mixture is stirred for 4 hours at 120° C. and then poured into 1.2 litres of 2N hydrochloric acid. The precipitate is filtered off, washed with water until neutral and dried in a vacuum drying chamber.

Aufarbeitung

  1. filtrationThe precipitate is filtered off
  2. washwashed with water until neutral and
  3. customdried in a vacuum
  4. customdrying chamber

Quellen und Nachweise

ORD-Eintrag
ord-ff4220b227644a7a8ebc840d4976dfa6
Quelldatensatz
uspto-grants-2008_11
Patentnummer
US07456316B2

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