Iodoethane → o-Diethoxybenzene

HRID 275734Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 275734
[CH2:1]([O:3][C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][C:5]=1[OH:10])[CH3:2].I[CH2:12][CH3:13].C(=O)([O-])[O-].[K+].[K+].C(OCC)(=O)C>CN(C)C=O>[CH2:1]([O:3][C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][C:5]=1[O:10][CH2:12][CH3:13])[CH3:2]

Komponenten

6

Edukt 4

HCID 6340IodoethaneHCID 8857Ethyl AcetateHCID 11430Potassium CarbonateHCID 667552-Ethoxyphenol

Produkt 1

HCID 74904o-Diethoxybenzene

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 6228DimethylformamideLösungsmittel

Reaktionsbedingungen

Temperatur
80 °C

Versuchsvorschrift

15.0 g of 2-ethoxyphenol, 18.0 ml of iodoethane and 30.0 g of potassium carbonate were suspended in 150 ml dimethylformamide, and the mixture was stirred at 80° C. for 30 hours. Ethyl acetate was added thereto, and the mixture was washed with water for five times and with brine, and then dried over anhydrous magnesium sulfate. The solvent was evaporated to give the title compound quantitatively as a red-brown oil.

Aufarbeitung

  1. washthe mixture was washed with water for five times and with brine
  2. dry with materialdried over anhydrous magnesium sulfate
  3. customThe solvent was evaporated

Quellen und Nachweise

ORD-Eintrag
ord-5e127ff570ff4237a3f13c93f6e9d430
Quelldatensatz
uspto-grants-2002_03
Patentnummer
US06352989B1

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