Chloroacetic Acid → 2-(2-Methyl-4-nitrophenylimino)-3-(2-methylbutyl)-1,3-thiazolidin-4-one

HRID 276667

Reaktionsgleichung

[CH3:1][C:2]1[CH:7]=[C:6]([N+:8]([O-:10])=[O:9])[CH:5]=[CH:4][C:3]=1[N:11]=[C:12]=[S:13].[CH3:14][CH:15]([CH2:18][CH3:19])[CH2:16][NH2:17].Cl[CH2:21][C:22](O)=[O:23]>>[CH3:1][C:2]1[CH:7]=[C:6]([N+:8]([O-:10])=[O:9])[CH:5]=[CH:4][C:3]=1[N:11]=[C:12]1[N:17]([CH2:16][CH:15]([CH3:14])[CH2:18][CH3:19])[C:22](=[O:23])[CH2:21][S:13]1

Komponenten

Edukt 3

HCID 300Chloroacetic Acid

HCID 72832-Methylbutylamine

HCID 1456212-Methyl-4-nitrophenyl isothiocyanate

Produkt 1

HCID 99449832-(2-Methyl-4-nitrophenylimino)-3-(2-methylbutyl)-1,3-thiazolidin-4-one

Versuchsvorschrift

2-Methyl-4-nitrophenyl isothiocyanate was reacted with 2-methyl-1-butylamine followed by chloroacetic acid according to Method C8a to afford 2-(2-methyl-4-nitrophenylimino)-3-(2-methylbutyl)-1,3-thiazolidin4-one.

Quellen und Nachweise

ORD-Eintrag: ord-2d21e540776a4d08bcf76c6c2c13dfd7
Quelldatensatz: uspto-grants-2002_03
DOI: 10.6084/m9.figshare.5104873.v1
Patentnummer: US06353006B1

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