Hydrazine hydrate (1:1) → Arabinosehydrazon

HRID 279931

Reaktionsgleichung

Reaktionsgleichung von HRID 279931
[O:1]=[CH:2][C@H:3]([C@@H:5]([C@@H:7]([CH2:9]O)[OH:8])[OH:6])[OH:4].O.[NH2:12][NH2:13]>CO>[CH:9](=[N:12][NH2:13])[C@H:7]([C@@H:5]([C@@H:3]([CH2:2][OH:1])[OH:4])[OH:6])[OH:8]

Komponenten

4

Edukt 2

HCID 24654Hydrazine hydrate (1:1)HCID 66308D-Arabinose

Produkt 1

HCID 86740783Arabinosehydrazon

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 887MethanolLösungsmittel

Versuchsvorschrift

A solution of 4.0 g of D-arabinose in 10 ml of methanol and 10 ml of hydrazine hydrate was stirred overnight, then evaporated to dryness in vacuo. The residue was triturated with 25 ml of methanol and the solid was collected, giving 3.5 g of D-arabinose hydrazone.

Aufarbeitung

  1. customevaporated to dryness in vacuo
  2. customThe residue was triturated with 25 ml of methanol
  3. customthe solid was collected

Quellen und Nachweise

ORD-Eintrag
ord-ebf88657c39e4ad8abc375b13788fe63
Quelldatensatz
uspto-grants-1986_05
Patentnummer
US04587331

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