HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Hydrochloric Acid → 4-Nitro-3-phenyl-L-alanine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Hydrochloric Acid | HCID 313 | — |
| Edukt | Nitric Acid | HCID 944 | — |
| Edukt | L-Phenylalanine | HCID 6140 | — |
| Lösungsmittel | Sulfuric Acid | HCID 1118 | — |
| Produkt | 4-Nitro-3-phenyl-L-alanine | HCID 13706 | 43% |
Reaktionsschritte
Using the procedure of Bergel and Stock as set forth in J. Chem. Soc., 2409-2417 (1954) L-phenylalanine (50 g) was treated with a mixture of concentrated sulfuric acid (150 ml), and fuming nitric acid (28 ml) to produce the nitro compound Yield 26.9 g (43%) mp 232°-234° C., [α]D25 =+9.6° (c=1.77, 1N HCl).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04587046 |
| Quelldatensatz | uspto-grants-1986_05 |
| ORD ID | ord-bcffd1e26f1f46a8acd5510ab76f2131 |
| Quellennotiz | uspto-grants-1986_05 |