Ethyl ketone → (2,2-Diethyl-1,3-dioxan-5-yl)methanol
Reaktionsgleichung
[OH:1][CH2:2][CH:3]([CH2:6][OH:7])[CH2:4][OH:5].[CH3:8][CH2:9][C:10](=O)[CH2:11][CH3:12]>>[CH2:9]([C:10]1([CH2:11][CH3:12])[O:5][CH2:4][CH:3]([CH2:6][OH:7])[CH2:2][O:1]1)[CH3:8]Komponenten
3
Versuchsvorschrift
The same procedure as in the step (7a) of Example 7 was repeated using 2-(hydroxymethyl)-1,3-propanediol, and 3-pentanone to obtain the title compound (1.5 g, yield: 46%) as a light yellow oil.
Quellen und Nachweise
- ORD-Eintrag
- ord-df690b281915412e85a8cfc989c8363c
- Quelldatensatz
- uspto-grants-2008_09
- Patentnummer
- US07425634B2
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