1-[4-(4-Hydroxyphenyl)butyl]imidazole → HCID 22009836, Verbindung

Beteiligte Stoffe

Rolle	Name	HCID	Einwaage
Edukt	1-[4-(4-Hydroxyphenyl)butyl]imidazole	HCID 22009664	—
Edukt	4-Chloromethyl-2-(3-methyl-2-thienyl)oxazole	HCID 22009832	—
Produkt	HCID 22009836	HCID 22009836	87%

Reaktionsschritte

In substantially the same manner as in Working Example 72, 1-[4-(4-hydroxyphenyl)butyl]imidazole was allowed to react with 4-chloromethyl-2-(3-methyl-2-thienyl)oxazole to give 4-[4-[4-(1-imidazolyl)butyl]phenoxymethyl]-2-(3-methyl-2-thienyl)oxazole. The yield was 87%. Recrystallization from ethyl acetate-hexane gave colorless prisms, mp 88-89° C.

Herkunft & Nachweise

DOI	10.6084/m9.figshare.5104873.v1
Patentnummer	US06211215B1
Quelldatensatz	uspto-grants-2001_04
ORD ID	ord-e1eaf52b0e264eadb26e5e3450bd0815
Quellennotiz	uspto-grants-2001_04