2-Propanone, 1-(3,4-dimethoxyphenyl)- → 3,4-Dma, (R)-

HRID 324949

Reaktionsgleichung

Reaktionsgleichung von HRID 324949
C(O)[C:2]([NH2:7])([CH2:5]O)[CH2:3]O.Cl.[CH3:10][O:11][C:12]1[CH:13]=[C:14](CC(=O)C)[CH:15]=[CH:16][C:17]=1[O:18][CH3:19].C1([C@H](N)C)C=CC=CC=1>>[CH3:10][O:11][C:12]1[CH:13]=[C:14]([CH2:5][C@H:2]([NH2:7])[CH3:3])[CH:15]=[CH:16][C:17]=1[O:18][CH3:19]

Komponenten

4

Edukt 3

HCID 698962-Propanone, 1-(3,4-dimethoxyphenyl)-HCID 93573Tromethamine hydrochlorideHCID 6431891-Phenethylamine, (+)-

Produkt 1

HCID 117694083,4-Dma, (R)-

Versuchsvorschrift

Using 10 ml of the cell-free extract, the components were reacted in 100 ml of a reaction mixture comprising a 0.1 M Tris-hydrochloric acid buffer (pH 8.5) containing 0.5 g of 1-(3,4-dimethoxyphenyl)-2-propanone and 0.34 g of (R)-1-phenylethylamine at 30° C. for 24 hours. As a result, 0.36 g of (R)-(3,4-dimethoxyphenyl)-2-aminopropane was formed.

Aufarbeitung

  1. extractionextract
  2. customthe components were reacted in 100 ml of a reaction mixture

Quellen und Nachweise

ORD-Eintrag
ord-457daacc5991415ab694fef18f9be7de
Quelldatensatz
uspto-grants-2001_04
Patentnummer
US06221638B1

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