2-Ethylbutyraldehyde → 3,7-Diethyl-5-azanona-3,5-diene

HRID 325979

Reaktionsgleichung

Reaktionsgleichung von HRID 325979
[OH-].[NH4+:2].[CH2:3]([CH:5]([CH2:8][CH3:9])[CH:6]=O)[CH3:4]>>[CH2:3]([C:5](=[CH:6][N:2]=[CH:6][CH:5]([CH2:8][CH3:9])[CH2:3][CH3:4])[CH2:8][CH3:9])[CH3:4]

Komponenten

3

Edukt 2

HCID 73592-EthylbutyraldehydeHCID 14923Ammonium Hydroxide

Produkt 1

HCID 124134703,7-Diethyl-5-azanona-3,5-dieneAusbeute 76,5 %

Versuchsvorschrift

To a sample of 250 grams of 28% ammonium hydroxide was added 215 grams of 2-ethylbutyraldehyde and the heterogeneous mixture was stirred for 18 hours at ambient temperature. The resulting organic layer was separated, and after drying, slowly distilled at atmospheric pressure to yield 148.8 grams of 3,7-diethyl-5-azanona-3,5-diene.

Aufarbeitung

  1. customThe resulting organic layer was separated
  2. customafter drying
  3. distillationslowly distilled at atmospheric pressure

Quellen und Nachweise

ORD-Eintrag
ord-7485e4e1d9c24c839b4ca499287abe82
Quelldatensatz
uspto-grants-1984_04
Patentnummer
US04443609

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