Acrylonitrile → 3-[(3-Hydroxypropyl)amino]propanenitrile

HRID 328182Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 328182
[NH2:1][CH2:2][CH2:3][CH2:4][OH:5].[C:6](#[N:9])[CH:7]=[CH2:8]>>[C:6]([CH2:7][CH2:8][NH:1][CH2:2][CH2:3][CH2:4][OH:5])#[N:9]

Komponenten

3

Edukt 2

HCID 7855AcrylonitrileHCID 90863-Amino-1-propanol

Produkt 1

HCID 135569403-[(3-Hydroxypropyl)amino]propanenitrile

Versuchsvorschrift

A solution of 75 g. (1 mole) of 3-aminopropanol is stirred while 54 g. (1 mole) of acrylonitrile is added dropwise. After being allowed to stand at room temperature for several hours and preferably overnight, the reaction mixture is concentrated under reduced pressure at 50° yielding 3-(2-cyanoethyl)aminopropanol.

Aufarbeitung

  1. concentrationthe reaction mixture is concentrated under reduced pressure at 50°

Quellen und Nachweise

ORD-Eintrag
ord-ec213696efae4142b407e4af2116f5ac
Quelldatensatz
uspto-grants-1977_04
Patentnummer
US04016209

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