1-Decene → 1-Tricosene

HRID 328187

Reaktionsgleichung

[CH2:1]=[CH:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH3:10].[CH3:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH:19]=[CH:20][CH2:21][CH2:22][CH2:23]CCCCC>>[CH2:1]=[CH:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:23][CH2:22][CH2:21][CH2:20][CH2:19][CH2:18][CH2:17][CH2:16][CH2:15][CH2:14][CH2:13][CH2:12][CH3:11]

Komponenten

Edukt 2

HCID 133811-Decene

HCID 521661CID 521661

Produkt 1

HCID 1811541-Tricosene

Versuchsvorschrift

Example 1 was repeated, with the difference that 20 ml. of 1-decene was utilized in place of 9-octadecene. Within 5 minutes, 4.8% by weight of tricosene was formed and within 30 minutes, 5.7% by weight of tricosene was obtained.

Quellen und Nachweise

ORD-Eintrag: ord-27e7f06a28f94b65bdd1209b8bfe4d71
Quelldatensatz: uspto-grants-1977_04
DOI: 10.6084/m9.figshare.5104873.v1
Patentnummer: US04016220

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